Official Methods of Analysis of AOAC INTERNATIONAL (22nd Edition)
Published:
04 January 2023
Online ISBN:
9780197610145
Print ISBN:
9780197610138
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Chapter
41.1.16
AOAC Official Method 965.33
Peroxide Value of Oils and Fats: Titration Method
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Page
C41-12
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Published:04 January 2023
Cite
'AOAC Official Method 965.33
Peroxide Value of Oils and Fats: Titration Method', in David Firestone, and Martin Peter Yurawecz (eds), Oils and Fats, in Dr. George W Latimer, Jr. (ed.), Official Methods of Analysis of AOAC INTERNATIONAL, 22nd Edition (New York , 2023; online edn, AOAC Publications, 4 Jan. 2023), https://doi.org/10.1093/9780197610145.003.3502, accessed 28 July 2026.
Peroxide Value of Oils and Fats: Titration Method', in David Firestone, and Martin Peter Yurawecz (eds), Oils and Fats, in Dr. George W Latimer, Jr. (ed.), Official Methods of Analysis of AOAC INTERNATIONAL, 22nd Edition (
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Extract
First Action 1965
Final Action 1969
AOCS–AOAC Method
(Note: Conduct analysis in diffuse daylight or in artificial light shielded from direct light source.)
Reagents
...
Determination
...
Conduct blank determination daily (must be ≤0.1 mL 0.1 M Na2S2O3). Subtract from test portion titration.
Peroxide value (milliequivalent peroxide/kg oil or fat) = S × M × 1000/g test portion, where S = mL Na2S2O3 (blank corrected) and M = molarity Na2S2O3 solution.
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