Table 3. Open in new tab Examination of... | Oxford Academic

Table 3.

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Examination of the stoichiometric ratio of compounds and flow rates.


Entry	X (equiv)	Y (equiv)	Z (mL/min)	W (mL/min)	HPLC-UV Yield of 3 (%)
1	2.5	1.0	2.0	1.2	77
2	1.5	1.0	2.0	1.2	77
3	1.2	1.0	2.0	1.2	84
4	1.0	1.0	2.0	1.2	74
5	1.0	1.2	2.0	1.2	88
6	1.0	1.5	2.0	1.2	90
7	1.0	2.0	2.0	1.2	85
8	1.0	2.5	2.0	1.2	86
9	1.0	1.5	1.2	2.0	86
10	1.0	1.5	1.6	1.6	89


Entry	X (equiv)	Y (equiv)	Z (mL/min)	W (mL/min)	HPLC-UV Yield of 3 (%)
1	2.5	1.0	2.0	1.2	77
2	1.5	1.0	2.0	1.2	77
3	1.2	1.0	2.0	1.2	84
4	1.0	1.0	2.0	1.2	74
5	1.0	1.2	2.0	1.2	88
6	1.0	1.5	2.0	1.2	90
7	1.0	2.0	2.0	1.2	85
8	1.0	2.5	2.0	1.2	86
9	1.0	1.5	1.2	2.0	86
10	1.0	1.5	1.6	1.6	89

Table 3.

Open in new tab

Examination of the stoichiometric ratio of compounds and flow rates.


Entry	X (equiv)	Y (equiv)	Z (mL/min)	W (mL/min)	HPLC-UV Yield of 3 (%)
1	2.5	1.0	2.0	1.2	77
2	1.5	1.0	2.0	1.2	77
3	1.2	1.0	2.0	1.2	84
4	1.0	1.0	2.0	1.2	74
5	1.0	1.2	2.0	1.2	88
6	1.0	1.5	2.0	1.2	90
7	1.0	2.0	2.0	1.2	85
8	1.0	2.5	2.0	1.2	86
9	1.0	1.5	1.2	2.0	86
10	1.0	1.5	1.6	1.6	89


Entry	X (equiv)	Y (equiv)	Z (mL/min)	W (mL/min)	HPLC-UV Yield of 3 (%)
1	2.5	1.0	2.0	1.2	77
2	1.5	1.0	2.0	1.2	77
3	1.2	1.0	2.0	1.2	84
4	1.0	1.0	2.0	1.2	74
5	1.0	1.2	2.0	1.2	88
6	1.0	1.5	2.0	1.2	90
7	1.0	2.0	2.0	1.2	85
8	1.0	2.5	2.0	1.2	86
9	1.0	1.5	1.2	2.0	86
10	1.0	1.5	1.6	1.6	89