Table 1

The XRD parameters of BBP in different voltages

Treatment2θ (°)FWHMGS (Å)d (Å)CL (%)
Control9.41 ± 0.02a2.78 ± 0.02e30.00 ± 0.67a9.16 ± 0.04f39.43 ± 0.12a
19.69 ± 0.03a8.24 ± 0.03e10.33 ± 0.67a4.51 ± 0.02d39.43 ± 0.12a
40 V9.41 ± 0.01a2.84 ± 0.03d28.00 ± 0.58abc9.40 ± 0.02d37.03 ± 0.24b
19.67 ± 0.01ab8.46 ± 0.02bc10.00 ± 0.00a4.51 ± 0.01cd37.03 ± 0.24b
80 V9.24 ± 0.02c2.96 ± 0.04c27.00 ± 1.15bcd9.58 ± 0.02c34.80 ± 0.40c
19.57 ± 0.01c8.76 ± 0.02b8.67 ± 0.33c4.54 ± 0.01b34.80 ± 0.40c
120 V9.09 ± 0.01d3.05 ± 0.02b26.00 ± 1.15cd9.73 ± 0.01b32.30 ± 0.23d
19.57 ± 0.02c8.74 ± 0.03b8.33 ± 0.67cd4.54 ± 0.01b32.30 ± 0.23d
160 V8.92 ± 0.03e3.07 ± 0.04b25.00 ± 0.58de9.91 ± 0.02a31.47 ± 0.44e
19.40 ± 0.03d8.67 ± 0.02b7.67 ± 0.33de4.58 ± 0.02a31.47 ± 0.44e
200 V8.90 ± 0.01e3.49 ± 0.04a23.00 ± 1.15e9.93 ± 0.05a27.93 ± 0.15f
19.40 ± 0.05d9.62 ± 0.07a7.00 ± 0.00e4.58 ± 0.01a27.93 ± 0.15f
Treatment2θ (°)FWHMGS (Å)d (Å)CL (%)
Control9.41 ± 0.02a2.78 ± 0.02e30.00 ± 0.67a9.16 ± 0.04f39.43 ± 0.12a
19.69 ± 0.03a8.24 ± 0.03e10.33 ± 0.67a4.51 ± 0.02d39.43 ± 0.12a
40 V9.41 ± 0.01a2.84 ± 0.03d28.00 ± 0.58abc9.40 ± 0.02d37.03 ± 0.24b
19.67 ± 0.01ab8.46 ± 0.02bc10.00 ± 0.00a4.51 ± 0.01cd37.03 ± 0.24b
80 V9.24 ± 0.02c2.96 ± 0.04c27.00 ± 1.15bcd9.58 ± 0.02c34.80 ± 0.40c
19.57 ± 0.01c8.76 ± 0.02b8.67 ± 0.33c4.54 ± 0.01b34.80 ± 0.40c
120 V9.09 ± 0.01d3.05 ± 0.02b26.00 ± 1.15cd9.73 ± 0.01b32.30 ± 0.23d
19.57 ± 0.02c8.74 ± 0.03b8.33 ± 0.67cd4.54 ± 0.01b32.30 ± 0.23d
160 V8.92 ± 0.03e3.07 ± 0.04b25.00 ± 0.58de9.91 ± 0.02a31.47 ± 0.44e
19.40 ± 0.03d8.67 ± 0.02b7.67 ± 0.33de4.58 ± 0.02a31.47 ± 0.44e
200 V8.90 ± 0.01e3.49 ± 0.04a23.00 ± 1.15e9.93 ± 0.05a27.93 ± 0.15f
19.40 ± 0.05d9.62 ± 0.07a7.00 ± 0.00e4.58 ± 0.01a27.93 ± 0.15f

2θ, diffraction angle; CL, relative crystallinity; FWHM, half-width height of diffraction peak; GS, granular size; d: lattice distance. The variable letters (a–e) appended to numerals reflected significant differences (P < 0.05).

Table 1

The XRD parameters of BBP in different voltages

Treatment2θ (°)FWHMGS (Å)d (Å)CL (%)
Control9.41 ± 0.02a2.78 ± 0.02e30.00 ± 0.67a9.16 ± 0.04f39.43 ± 0.12a
19.69 ± 0.03a8.24 ± 0.03e10.33 ± 0.67a4.51 ± 0.02d39.43 ± 0.12a
40 V9.41 ± 0.01a2.84 ± 0.03d28.00 ± 0.58abc9.40 ± 0.02d37.03 ± 0.24b
19.67 ± 0.01ab8.46 ± 0.02bc10.00 ± 0.00a4.51 ± 0.01cd37.03 ± 0.24b
80 V9.24 ± 0.02c2.96 ± 0.04c27.00 ± 1.15bcd9.58 ± 0.02c34.80 ± 0.40c
19.57 ± 0.01c8.76 ± 0.02b8.67 ± 0.33c4.54 ± 0.01b34.80 ± 0.40c
120 V9.09 ± 0.01d3.05 ± 0.02b26.00 ± 1.15cd9.73 ± 0.01b32.30 ± 0.23d
19.57 ± 0.02c8.74 ± 0.03b8.33 ± 0.67cd4.54 ± 0.01b32.30 ± 0.23d
160 V8.92 ± 0.03e3.07 ± 0.04b25.00 ± 0.58de9.91 ± 0.02a31.47 ± 0.44e
19.40 ± 0.03d8.67 ± 0.02b7.67 ± 0.33de4.58 ± 0.02a31.47 ± 0.44e
200 V8.90 ± 0.01e3.49 ± 0.04a23.00 ± 1.15e9.93 ± 0.05a27.93 ± 0.15f
19.40 ± 0.05d9.62 ± 0.07a7.00 ± 0.00e4.58 ± 0.01a27.93 ± 0.15f
Treatment2θ (°)FWHMGS (Å)d (Å)CL (%)
Control9.41 ± 0.02a2.78 ± 0.02e30.00 ± 0.67a9.16 ± 0.04f39.43 ± 0.12a
19.69 ± 0.03a8.24 ± 0.03e10.33 ± 0.67a4.51 ± 0.02d39.43 ± 0.12a
40 V9.41 ± 0.01a2.84 ± 0.03d28.00 ± 0.58abc9.40 ± 0.02d37.03 ± 0.24b
19.67 ± 0.01ab8.46 ± 0.02bc10.00 ± 0.00a4.51 ± 0.01cd37.03 ± 0.24b
80 V9.24 ± 0.02c2.96 ± 0.04c27.00 ± 1.15bcd9.58 ± 0.02c34.80 ± 0.40c
19.57 ± 0.01c8.76 ± 0.02b8.67 ± 0.33c4.54 ± 0.01b34.80 ± 0.40c
120 V9.09 ± 0.01d3.05 ± 0.02b26.00 ± 1.15cd9.73 ± 0.01b32.30 ± 0.23d
19.57 ± 0.02c8.74 ± 0.03b8.33 ± 0.67cd4.54 ± 0.01b32.30 ± 0.23d
160 V8.92 ± 0.03e3.07 ± 0.04b25.00 ± 0.58de9.91 ± 0.02a31.47 ± 0.44e
19.40 ± 0.03d8.67 ± 0.02b7.67 ± 0.33de4.58 ± 0.02a31.47 ± 0.44e
200 V8.90 ± 0.01e3.49 ± 0.04a23.00 ± 1.15e9.93 ± 0.05a27.93 ± 0.15f
19.40 ± 0.05d9.62 ± 0.07a7.00 ± 0.00e4.58 ± 0.01a27.93 ± 0.15f

2θ, diffraction angle; CL, relative crystallinity; FWHM, half-width height of diffraction peak; GS, granular size; d: lattice distance. The variable letters (a–e) appended to numerals reflected significant differences (P < 0.05).

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