Effect of the Number of Days and Repetitions on False Acceptance and False Rejection Rate for Experimental Designs With Three Samples
| . | Between-Day Imprecision . | . | . | Repeatability . | . | . | Between-Day Imprecision . | . | . | Repeatability . | . | . |
|---|---|---|---|---|---|---|---|---|---|---|---|---|
| . | False Acceptance Rate, % . | . | . | . | . | . | False Rejection Rate, % . | . | . | . | . | . |
| No. of Replicates . | 5 Days × nrep . | . | . | . | . | . | . | . | . | . | . | . |
| . | Actual Factor of Increase From Claimed Value . | . | . | . | . | . | Observed Factor of Increase From Claimed Value . | . | . | . | . | . |
| . | 1.1 . | 1.2 . | 1.5 . | 1.1 . | 1.2 . | 1.5 . | ≥1.1 . | ≥1.2 . | ≥1.5 . | ≥1.1 . | ≥1.2 . | ≥1.5 . |
| 2 | 14.1 | 8.8 | 2.2 | 98.4 | 95.2 | 69.6 | 66.3 | 54.2 | 22.2 | 65.9 | 50.0 | 13.4 |
| 3 | 14.1 | 8.8 | 2.2 | 76.5 | 55.5 | 9.6 | 66.3 | 54.2 | 22.2 | 62.4 | 39.8 | 3.8 |
| 4 | 14.1 | 8.8 | 2.2 | 27.7 | 10.1 | 0.2 | 66.3 | 54.2 | 22.2 | 58.6 | 31.6 | 1.1 |
| 5 | 14.1 | 8.8 | 2.2 | 3.2 | 0.4 | 0.0 | 66.3 | 54.2 | 22.2 | 55.0 | 25.1 | 0.3 |
| 6 | 14.1 | 8.8 | 2.2 | 0.1 | 0.0 | 0.0 | 66.3 | 54.2 | 22.2 | 51.6 | 20.0 | 0.1 |
| 7 | 4.3 | 2.2 | 0.3 | 0.0 | 0.0 | 0.0 | 66.3 | 52.1 | 17.2 | 48.5 | 15.9 | 0.0 |
| 20 | 4.3 | 2.2 | 0.3 | 0.0 | 0.0 | 0.0 | 66.3 | 52.1 | 17.2 | 22.2 | 1.0 | 0.0 |
| No. of Days | nday × 5 Replicates | |||||||||||
| 2 | 69.2 | 61.6 | 42.5 | 89.7 | 76.7 | 27.2 | 61.3 | 54.4 | 35.0 | 63.9 | 43.6 | 6.2 |
| 3 | 35.9 | 27.1 | 11.5 | 57.6 | 33.2 | 2.4 | 65.4 | 55.6 | 28.4 | 60.9 | 36.3 | 2.3 |
| 4 | 14.1 | 8.8 | 2.2 | 19.8 | 6.1 | 0.1 | 66.3 | 54.2 | 22.2 | 57.9 | 30.1 | 0.9 |
| 5 | 14.1 | 8.8 | 2.2 | 3.2 | 0.4 | 0.0 | 66.3 | 54.2 | 22.2 | 55.0 | 25.1 | 0.3 |
| 6 | 4.3 | 2.2 | 0.3 | 0.2 | 0.0 | 0.0 | 66.3 | 52.1 | 17.2 | 52.3 | 20.9 | 0.1 |
| 7 | 1.1 | 0.4 | 0.0 | 0.0 | 0.0 | 0.0 | 65.9 | 50.0 | 13.4 | 49.7 | 17.4 | 0.0 |
| 20 | 0.0 | 0.0 | 0.0 | 0.0 | 0.0 | 0.0 | 57.9 | 30.1 | 0.9 | 26.4 | 1.8 | 0.0 |
| . | Between-Day Imprecision . | . | . | Repeatability . | . | . | Between-Day Imprecision . | . | . | Repeatability . | . | . |
|---|---|---|---|---|---|---|---|---|---|---|---|---|
| . | False Acceptance Rate, % . | . | . | . | . | . | False Rejection Rate, % . | . | . | . | . | . |
| No. of Replicates . | 5 Days × nrep . | . | . | . | . | . | . | . | . | . | . | . |
| . | Actual Factor of Increase From Claimed Value . | . | . | . | . | . | Observed Factor of Increase From Claimed Value . | . | . | . | . | . |
| . | 1.1 . | 1.2 . | 1.5 . | 1.1 . | 1.2 . | 1.5 . | ≥1.1 . | ≥1.2 . | ≥1.5 . | ≥1.1 . | ≥1.2 . | ≥1.5 . |
| 2 | 14.1 | 8.8 | 2.2 | 98.4 | 95.2 | 69.6 | 66.3 | 54.2 | 22.2 | 65.9 | 50.0 | 13.4 |
| 3 | 14.1 | 8.8 | 2.2 | 76.5 | 55.5 | 9.6 | 66.3 | 54.2 | 22.2 | 62.4 | 39.8 | 3.8 |
| 4 | 14.1 | 8.8 | 2.2 | 27.7 | 10.1 | 0.2 | 66.3 | 54.2 | 22.2 | 58.6 | 31.6 | 1.1 |
| 5 | 14.1 | 8.8 | 2.2 | 3.2 | 0.4 | 0.0 | 66.3 | 54.2 | 22.2 | 55.0 | 25.1 | 0.3 |
| 6 | 14.1 | 8.8 | 2.2 | 0.1 | 0.0 | 0.0 | 66.3 | 54.2 | 22.2 | 51.6 | 20.0 | 0.1 |
| 7 | 4.3 | 2.2 | 0.3 | 0.0 | 0.0 | 0.0 | 66.3 | 52.1 | 17.2 | 48.5 | 15.9 | 0.0 |
| 20 | 4.3 | 2.2 | 0.3 | 0.0 | 0.0 | 0.0 | 66.3 | 52.1 | 17.2 | 22.2 | 1.0 | 0.0 |
| No. of Days | nday × 5 Replicates | |||||||||||
| 2 | 69.2 | 61.6 | 42.5 | 89.7 | 76.7 | 27.2 | 61.3 | 54.4 | 35.0 | 63.9 | 43.6 | 6.2 |
| 3 | 35.9 | 27.1 | 11.5 | 57.6 | 33.2 | 2.4 | 65.4 | 55.6 | 28.4 | 60.9 | 36.3 | 2.3 |
| 4 | 14.1 | 8.8 | 2.2 | 19.8 | 6.1 | 0.1 | 66.3 | 54.2 | 22.2 | 57.9 | 30.1 | 0.9 |
| 5 | 14.1 | 8.8 | 2.2 | 3.2 | 0.4 | 0.0 | 66.3 | 54.2 | 22.2 | 55.0 | 25.1 | 0.3 |
| 6 | 4.3 | 2.2 | 0.3 | 0.2 | 0.0 | 0.0 | 66.3 | 52.1 | 17.2 | 52.3 | 20.9 | 0.1 |
| 7 | 1.1 | 0.4 | 0.0 | 0.0 | 0.0 | 0.0 | 65.9 | 50.0 | 13.4 | 49.7 | 17.4 | 0.0 |
| 20 | 0.0 | 0.0 | 0.0 | 0.0 | 0.0 | 0.0 | 57.9 | 30.1 | 0.9 | 26.4 | 1.8 | 0.0 |
Effect of the Number of Days and Repetitions on False Acceptance and False Rejection Rate for Experimental Designs With Three Samples
| . | Between-Day Imprecision . | . | . | Repeatability . | . | . | Between-Day Imprecision . | . | . | Repeatability . | . | . |
|---|---|---|---|---|---|---|---|---|---|---|---|---|
| . | False Acceptance Rate, % . | . | . | . | . | . | False Rejection Rate, % . | . | . | . | . | . |
| No. of Replicates . | 5 Days × nrep . | . | . | . | . | . | . | . | . | . | . | . |
| . | Actual Factor of Increase From Claimed Value . | . | . | . | . | . | Observed Factor of Increase From Claimed Value . | . | . | . | . | . |
| . | 1.1 . | 1.2 . | 1.5 . | 1.1 . | 1.2 . | 1.5 . | ≥1.1 . | ≥1.2 . | ≥1.5 . | ≥1.1 . | ≥1.2 . | ≥1.5 . |
| 2 | 14.1 | 8.8 | 2.2 | 98.4 | 95.2 | 69.6 | 66.3 | 54.2 | 22.2 | 65.9 | 50.0 | 13.4 |
| 3 | 14.1 | 8.8 | 2.2 | 76.5 | 55.5 | 9.6 | 66.3 | 54.2 | 22.2 | 62.4 | 39.8 | 3.8 |
| 4 | 14.1 | 8.8 | 2.2 | 27.7 | 10.1 | 0.2 | 66.3 | 54.2 | 22.2 | 58.6 | 31.6 | 1.1 |
| 5 | 14.1 | 8.8 | 2.2 | 3.2 | 0.4 | 0.0 | 66.3 | 54.2 | 22.2 | 55.0 | 25.1 | 0.3 |
| 6 | 14.1 | 8.8 | 2.2 | 0.1 | 0.0 | 0.0 | 66.3 | 54.2 | 22.2 | 51.6 | 20.0 | 0.1 |
| 7 | 4.3 | 2.2 | 0.3 | 0.0 | 0.0 | 0.0 | 66.3 | 52.1 | 17.2 | 48.5 | 15.9 | 0.0 |
| 20 | 4.3 | 2.2 | 0.3 | 0.0 | 0.0 | 0.0 | 66.3 | 52.1 | 17.2 | 22.2 | 1.0 | 0.0 |
| No. of Days | nday × 5 Replicates | |||||||||||
| 2 | 69.2 | 61.6 | 42.5 | 89.7 | 76.7 | 27.2 | 61.3 | 54.4 | 35.0 | 63.9 | 43.6 | 6.2 |
| 3 | 35.9 | 27.1 | 11.5 | 57.6 | 33.2 | 2.4 | 65.4 | 55.6 | 28.4 | 60.9 | 36.3 | 2.3 |
| 4 | 14.1 | 8.8 | 2.2 | 19.8 | 6.1 | 0.1 | 66.3 | 54.2 | 22.2 | 57.9 | 30.1 | 0.9 |
| 5 | 14.1 | 8.8 | 2.2 | 3.2 | 0.4 | 0.0 | 66.3 | 54.2 | 22.2 | 55.0 | 25.1 | 0.3 |
| 6 | 4.3 | 2.2 | 0.3 | 0.2 | 0.0 | 0.0 | 66.3 | 52.1 | 17.2 | 52.3 | 20.9 | 0.1 |
| 7 | 1.1 | 0.4 | 0.0 | 0.0 | 0.0 | 0.0 | 65.9 | 50.0 | 13.4 | 49.7 | 17.4 | 0.0 |
| 20 | 0.0 | 0.0 | 0.0 | 0.0 | 0.0 | 0.0 | 57.9 | 30.1 | 0.9 | 26.4 | 1.8 | 0.0 |
| . | Between-Day Imprecision . | . | . | Repeatability . | . | . | Between-Day Imprecision . | . | . | Repeatability . | . | . |
|---|---|---|---|---|---|---|---|---|---|---|---|---|
| . | False Acceptance Rate, % . | . | . | . | . | . | False Rejection Rate, % . | . | . | . | . | . |
| No. of Replicates . | 5 Days × nrep . | . | . | . | . | . | . | . | . | . | . | . |
| . | Actual Factor of Increase From Claimed Value . | . | . | . | . | . | Observed Factor of Increase From Claimed Value . | . | . | . | . | . |
| . | 1.1 . | 1.2 . | 1.5 . | 1.1 . | 1.2 . | 1.5 . | ≥1.1 . | ≥1.2 . | ≥1.5 . | ≥1.1 . | ≥1.2 . | ≥1.5 . |
| 2 | 14.1 | 8.8 | 2.2 | 98.4 | 95.2 | 69.6 | 66.3 | 54.2 | 22.2 | 65.9 | 50.0 | 13.4 |
| 3 | 14.1 | 8.8 | 2.2 | 76.5 | 55.5 | 9.6 | 66.3 | 54.2 | 22.2 | 62.4 | 39.8 | 3.8 |
| 4 | 14.1 | 8.8 | 2.2 | 27.7 | 10.1 | 0.2 | 66.3 | 54.2 | 22.2 | 58.6 | 31.6 | 1.1 |
| 5 | 14.1 | 8.8 | 2.2 | 3.2 | 0.4 | 0.0 | 66.3 | 54.2 | 22.2 | 55.0 | 25.1 | 0.3 |
| 6 | 14.1 | 8.8 | 2.2 | 0.1 | 0.0 | 0.0 | 66.3 | 54.2 | 22.2 | 51.6 | 20.0 | 0.1 |
| 7 | 4.3 | 2.2 | 0.3 | 0.0 | 0.0 | 0.0 | 66.3 | 52.1 | 17.2 | 48.5 | 15.9 | 0.0 |
| 20 | 4.3 | 2.2 | 0.3 | 0.0 | 0.0 | 0.0 | 66.3 | 52.1 | 17.2 | 22.2 | 1.0 | 0.0 |
| No. of Days | nday × 5 Replicates | |||||||||||
| 2 | 69.2 | 61.6 | 42.5 | 89.7 | 76.7 | 27.2 | 61.3 | 54.4 | 35.0 | 63.9 | 43.6 | 6.2 |
| 3 | 35.9 | 27.1 | 11.5 | 57.6 | 33.2 | 2.4 | 65.4 | 55.6 | 28.4 | 60.9 | 36.3 | 2.3 |
| 4 | 14.1 | 8.8 | 2.2 | 19.8 | 6.1 | 0.1 | 66.3 | 54.2 | 22.2 | 57.9 | 30.1 | 0.9 |
| 5 | 14.1 | 8.8 | 2.2 | 3.2 | 0.4 | 0.0 | 66.3 | 54.2 | 22.2 | 55.0 | 25.1 | 0.3 |
| 6 | 4.3 | 2.2 | 0.3 | 0.2 | 0.0 | 0.0 | 66.3 | 52.1 | 17.2 | 52.3 | 20.9 | 0.1 |
| 7 | 1.1 | 0.4 | 0.0 | 0.0 | 0.0 | 0.0 | 65.9 | 50.0 | 13.4 | 49.7 | 17.4 | 0.0 |
| 20 | 0.0 | 0.0 | 0.0 | 0.0 | 0.0 | 0.0 | 57.9 | 30.1 | 0.9 | 26.4 | 1.8 | 0.0 |
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