Table 4.

Tentatively identified major compounds of the resin shown in Fig. 4B

Retention time (min)Tentatively identified volatile compounds
15·972Copaene
18·5424,11,11-Trimethyl-8-methylene-bicyclo[7·2.0]undec-4-ene
19·059[1S-(1α,2β,4β)]-1-Ethenyl-1-methyl-2,4-bis(1-methylethenyl)-cyclohexane
19·221Caryophyllene
19·535(–)-Aristolene
21·415Humulene
21·6072-Isopropenyl-4a,8-dimethyl-1,2,3,4,4α,5,6,7-octahydronaphthalene
22·63[1S-(1α,7α,8aα)]-1,2,3,5,6,7,8,8α-Octahydro-1,8a-dimethyl-7-(1-methylethenyl)-naphthalene
22·877[1S-(1α,2β,4β]-1-Ethenyl-1-methyl-2,4-bis(1-methylethenyl)-cyclohexane
23·056[2R-(2α,4aα,8αβ)]-1,2,3,4,4a,5,6,8α-Octahydro-4α,8-dimethyl-2-(1-methylethenyl)-naphthalene,
24·025(1S-cis)-1,2,3,5,6,8a-Hexahydro-4,7-dimethyl-1-(1-methylethyl)-naphthalene
25·035α-Muurolene
28·9593,7,11,15-Tetramethyl-2-hexadecen-1-ol
29·156Cubedol
30·258Caryophyllene oxide
31·8073,7,11-Trimethyl-1,6,10-dodecatrien-3-ol
32·0311-Hydroxy-1,7-dimethyl-4-isopropyl-2,7-cyclodecadiene
35·0132-Isopropyl-5-methyl-9-methylene-bicyclo[4·4.0]dec-1-ene
36·466α-Cadinol
38·331Heneicosane
Retention time (min)Tentatively identified volatile compounds
15·972Copaene
18·5424,11,11-Trimethyl-8-methylene-bicyclo[7·2.0]undec-4-ene
19·059[1S-(1α,2β,4β)]-1-Ethenyl-1-methyl-2,4-bis(1-methylethenyl)-cyclohexane
19·221Caryophyllene
19·535(–)-Aristolene
21·415Humulene
21·6072-Isopropenyl-4a,8-dimethyl-1,2,3,4,4α,5,6,7-octahydronaphthalene
22·63[1S-(1α,7α,8aα)]-1,2,3,5,6,7,8,8α-Octahydro-1,8a-dimethyl-7-(1-methylethenyl)-naphthalene
22·877[1S-(1α,2β,4β]-1-Ethenyl-1-methyl-2,4-bis(1-methylethenyl)-cyclohexane
23·056[2R-(2α,4aα,8αβ)]-1,2,3,4,4a,5,6,8α-Octahydro-4α,8-dimethyl-2-(1-methylethenyl)-naphthalene,
24·025(1S-cis)-1,2,3,5,6,8a-Hexahydro-4,7-dimethyl-1-(1-methylethyl)-naphthalene
25·035α-Muurolene
28·9593,7,11,15-Tetramethyl-2-hexadecen-1-ol
29·156Cubedol
30·258Caryophyllene oxide
31·8073,7,11-Trimethyl-1,6,10-dodecatrien-3-ol
32·0311-Hydroxy-1,7-dimethyl-4-isopropyl-2,7-cyclodecadiene
35·0132-Isopropyl-5-methyl-9-methylene-bicyclo[4·4.0]dec-1-ene
36·466α-Cadinol
38·331Heneicosane

By comparison with the commercial NIST spectral mass library (NIST 1).

Table 4.

Tentatively identified major compounds of the resin shown in Fig. 4B

Retention time (min)Tentatively identified volatile compounds
15·972Copaene
18·5424,11,11-Trimethyl-8-methylene-bicyclo[7·2.0]undec-4-ene
19·059[1S-(1α,2β,4β)]-1-Ethenyl-1-methyl-2,4-bis(1-methylethenyl)-cyclohexane
19·221Caryophyllene
19·535(–)-Aristolene
21·415Humulene
21·6072-Isopropenyl-4a,8-dimethyl-1,2,3,4,4α,5,6,7-octahydronaphthalene
22·63[1S-(1α,7α,8aα)]-1,2,3,5,6,7,8,8α-Octahydro-1,8a-dimethyl-7-(1-methylethenyl)-naphthalene
22·877[1S-(1α,2β,4β]-1-Ethenyl-1-methyl-2,4-bis(1-methylethenyl)-cyclohexane
23·056[2R-(2α,4aα,8αβ)]-1,2,3,4,4a,5,6,8α-Octahydro-4α,8-dimethyl-2-(1-methylethenyl)-naphthalene,
24·025(1S-cis)-1,2,3,5,6,8a-Hexahydro-4,7-dimethyl-1-(1-methylethyl)-naphthalene
25·035α-Muurolene
28·9593,7,11,15-Tetramethyl-2-hexadecen-1-ol
29·156Cubedol
30·258Caryophyllene oxide
31·8073,7,11-Trimethyl-1,6,10-dodecatrien-3-ol
32·0311-Hydroxy-1,7-dimethyl-4-isopropyl-2,7-cyclodecadiene
35·0132-Isopropyl-5-methyl-9-methylene-bicyclo[4·4.0]dec-1-ene
36·466α-Cadinol
38·331Heneicosane
Retention time (min)Tentatively identified volatile compounds
15·972Copaene
18·5424,11,11-Trimethyl-8-methylene-bicyclo[7·2.0]undec-4-ene
19·059[1S-(1α,2β,4β)]-1-Ethenyl-1-methyl-2,4-bis(1-methylethenyl)-cyclohexane
19·221Caryophyllene
19·535(–)-Aristolene
21·415Humulene
21·6072-Isopropenyl-4a,8-dimethyl-1,2,3,4,4α,5,6,7-octahydronaphthalene
22·63[1S-(1α,7α,8aα)]-1,2,3,5,6,7,8,8α-Octahydro-1,8a-dimethyl-7-(1-methylethenyl)-naphthalene
22·877[1S-(1α,2β,4β]-1-Ethenyl-1-methyl-2,4-bis(1-methylethenyl)-cyclohexane
23·056[2R-(2α,4aα,8αβ)]-1,2,3,4,4a,5,6,8α-Octahydro-4α,8-dimethyl-2-(1-methylethenyl)-naphthalene,
24·025(1S-cis)-1,2,3,5,6,8a-Hexahydro-4,7-dimethyl-1-(1-methylethyl)-naphthalene
25·035α-Muurolene
28·9593,7,11,15-Tetramethyl-2-hexadecen-1-ol
29·156Cubedol
30·258Caryophyllene oxide
31·8073,7,11-Trimethyl-1,6,10-dodecatrien-3-ol
32·0311-Hydroxy-1,7-dimethyl-4-isopropyl-2,7-cyclodecadiene
35·0132-Isopropyl-5-methyl-9-methylene-bicyclo[4·4.0]dec-1-ene
36·466α-Cadinol
38·331Heneicosane

By comparison with the commercial NIST spectral mass library (NIST 1).

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